View this page in : French Dutch English
 
  SEARCH

 
Home > Business Sectors > Laboratories > NRL methods
Home About the FASFC Contact Business Sectors Animal production Approvals, authorisations and registrations Autocontrole (Self-checking) Checklists "Inspection" Compulsory Notification Export to third countries Foodstuffs Import from third countries Laboratories Plant production Advisory Committee Scientific Committee Publications

 
 

NRL methods



Dioxines (PCDD/PCDF) and PCB

Food Contact Materials (migration analyses & analysis of food in contact with-)

Heavy metals and trace elements

Marine toxins

Melamine

Microbiology

Mycotoxins

Pesticides residues

Polycyclic aromatic hydrocarbons (PAH)

Detection of inhibitors in raw milk

Veterinary drugs residues





Dioxines (PCDD/PCDF) and PCB

Date Subject Documents
24/12/2014 Extraction according to EN16215:2012 for sepiolite : robustness of extraction by ASE and purification with PowerPrep (by CART)

Validation file (Fr)

06/08/2014 Analyses of perfluorated compounds (PFAs) in food of animal origin by LC-MSMS. (by ISP-WIV)

Method (Fr)

Validation file (Fr)

31/12/2013 Analyses of dioxins (PCDD), furans (PCDF) and dioxin-like PCB in vegetable oil by GC-MS/MS (by CART)

Method (Fr)

Validation file (Fr)


Top of the page    




Food Contact Materials

Date Subject Documents
05/03/2015 Analysis of BADGE and derivatives in tuna fish by UPLC-FLUO (by ISP-WIV)

Method (Fr)

Validation file (Fr)

20/06/2014

Multi-element analyses in various stimulants by ICP-MS (by ISP-WIV)

Operating procedure for release testing In accordance with the Council of Europe Resolution CM/Res(2013)9 on metals and alloys used in food contact materials and articles

Validation dossier 1 : multi-element analyses by  ICP-MS in citric acid solutions (5 g/L) following contact with metallic objects

Validation dossier 2 : multi-element analyses by  ICP-MS in acetic acid solutions (3%) following contact with plastic and metallic objects

Validation dossier 3 : multi-element analyses by  ICP-MS in artificial tap water (ATW) following contact with metallic objects

Method (Fr)

 

 Operating procedure – metallic objects (Fr)

 

Validation file 1 (Fr)

 

Validation file 2  (Fr)

 

Validation file 3 (Fr)

06/08/2014 Analyses of photo-initators in food stimulant E (Tenax) after contact with food packaging material. (by ISP-WIV)

Method (Fr)

Validation file (Fr)

06/08/2014 Determination of photo-initiators in dry foods by UPLC-MS/MS (by ISP-WIV)

Method (Fr)

Validation file (Fr)

06/08/2014 Determination of Bisphenol A in water, 50% ethanol, 95% ethanol exposed to kitchen utensils made of polycarbonate (par l'ISP)

Method (Fr)

Validation file (Fr)

06/08/2014 Determination Phtalates in milk and babyfood by GC-MS (by ISP-WIV)

Method (Fr)

Validation file (Fr)

19/06/2014 Analyse des amines primaires aromatiques (26 composants) dans le liquide de contact (simulant B) ayant été mis en contact avec les ustensiles de cuisines en polyamide par (par l'ISP)

Method (Fr)

Validation file (Fr)

04/04/2014 Analysis of aluminum in citric acid (5 g/L) and artificial tap water (ATW) by ICP-AES according to CM/Res(2013)9 (by ISP-WIV)

Method (Fr)

Validation file (citric acid)

(Fr)

Validation file (ATW) (Fr)

02/10/2013 ESBO in food preserved in jars (by ISP-WIV)

Method (Fr)

Validation file (Fr)

04/09/2013 Determination of semicarbazide in foodstuffs (by ISP-WIV)

Method (Fr)

Validation file (Fr)

23/08/2012 Analysis of tin byICP-MS of food stimulants exposed to silicon food contact material (by ISP-WIV)

Method (Fr)

Validation file (Fr)

23/08/2012 Analysis of formaldehyde in liquid substances (food stimulant B) having been in contact with melamine kitchenware (by ISP-WIV)

Method (Fr)

Validation file (Fr)

01/04/2011 Analysis of photo-initiators in liquid substances (food simulants) having been in contact with packaging material (by ISP-WIV, v2)

Method (PDF)

Validation file (PDF)

25/03/2009 Determination of benzophenone and methylbenzophenone in cereals by means of GC-MSn (by ISP-WIV)

Method (Fr)

Validation file (Fr)

16/02/2009 Determination of benzophenone and methylbenzophenone in food by means of UPLC-MS/MS (by SGS)

Method

Validation file


Top of the page    



Heavy metals and trace elements

Date Subject Documents
18/06/2014 Determination of inorganic arsenic in foods, feed and drinks of vegetable origin (terrestrial plants) by HPLC-ICP-MS (v2, by CODA-CERVA)

Method (Du-Fr)

Validation dossier

11/02/2014 Determination of arsenic (As), cadmium (Cd), cupper (Cu), lead (Pb) and Zinc (Zn) in foodstuffs by ICP-MS (validation dossier, part Pb in milk products) (by CODA-CERVA)

Method (Du-Fr)

Validation dossier

11/02/2014 Determination of selenomethionine  and/or selenite in food supplements and feed premixtures (v1, CODA-CERVA)

Method (Du-Fr)

Validation dossier

06/06/2013 Extraction an isolation of inorganic arsenic in food of plant origin with  Solid Phase Extraction-SPE cartridges). (v1, CODA-CERVA)

Method (Du)

31/10/2012 Determination of As species in cereals and cereal products (by CERVA-CODA)
 

Method V2

Method V3 (Fr)

Validation file


Top of the page    



Marine toxins

Date Subject Documents
08/01/2014 Determination of PSP toxins by HPLC-fluorescence (AOAC 2005_06)

Validation dossier (WIV) (Du)

Validation dossier (CER) (Fr)

07/12/2011 Determination of lipophilic toxins by UPLC-MS/MS (by WIV-ISP, v3)

Method (Du)

Validation dossier (Du)


Top of the page    



Melamine

Date Subject Documents
04/08/2010 Determination of melamine by UPLC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation dossier (Fr)


Top of the page    



Microbiology

Date Subject Documents
17/06/2013 Detection of ESBL E.coli in veal, beef and porc Method (PDF)
30/05/2013

Enumeration of ESBL E.coli in chicken carcasses

Method (PDF)

Validation dossier (Fr)


Top of the page    



Mycotoxins

Date Subject Documents
11/02/2014

Determination by LC-MS/MS of patuline in fruits and derived products. (by CERVA-CODA)

 

Method (Fr)

Validation file (Fr)

11/02/2014

Determination by LC-MS/MS of aflatoxins AFB1, AFB2, AFG1, AFG2 and ochratoxin A (OTA) in spices, cocoa and cocoa derived product. (by CERVA-CODA)

Method (Fr)

Validation file (Fr)

22/03/2013

Dosage par HPLC-MS/MS des mycotoxines DON, ZEA, T-2, HT-2, OTA et AfB1, AfB2, AfG1, AfG2 dans des céréales et des produits dérivés (v6, par le CERVA)

Method (Fr)

Validation file (Fr)

22/03/2013

Determination of ochratoxine A in kidney, liver, and black pudding by UPLC-MS/MS (by CERVA-CODA)

Method (Fr)

Validation file (Fr)

22/03/2013

Multi-mycotoxin method for the simultaneous determination of 12 mycotoxins in rice, corn, and pistachios (by CERVA-CODA)

Method (Du)

Validation file (Du)


Top of the page    



Pesticides residues

Date Subject Documents
19/06/2014 Determination of chlormequat in milk by LC-MS/MS (by WIV-ISP)

Method (Fr)

Validation file (Fr)

19/06/2014 Determination of maleic hydrazide in milk by LC-MS/MS (by WIV-ISP)

Method (Fr)

Validation file (Fr)

19/06/2014 Determination of glyphosate in liver by UPLC-MS/MS (by ISP-WIV)

Method (Fr)

Validation file (Fr)

19/06/2014 Determination of pyrethroids in fat by LC-MS/MS (by ISP-WIV)

Method (Fr)

Validation file (Fr)

06/03/2013 Determination of etephon in fruits and vegetables by LC-MS/MS (by WIV-ISP)

Method (Fr)

Validation file (Fr)

31/01/2013 Mutlti-residue method for the determination of pesticide residues with GC-MS/MS in plant matrices with high protein or starch contents (by WIV-ISP)

Method (Fr)

MS/MS transition (Fr)

Validation file (Fr)

31/01/2013 Determination of maleic hydrazide in fruits and vegetables by LC-MS/MS (by WIV-ISP)

Method (Fr)

Validation file (Fr)

01/06/2011 Determination of glyphosate and glyphosate metabolites in food of plant origin by UPLC-MS/MS (by ISP-WIV)

Method (Fr)

MS/MS transition (Fr)

Validation dossier (Fr)

01/04/2011 Determination of amitraz and amitraz degradation products in fruit and vegetables by UPLC-MS/MS (by ISP-WIV)

Mehod (Fr)

MS/MS transition (Fr)

Validation dossier (Fr)

04/08/2010 Determination of pyrethroids by GC-ECD (by ISP-WIV)

Method (Fr)

Scope (Fr)

Validation dossier (Fr)

04/08/2010 Determination of organophosphorous pesticides by GC-MS/MS (by ISP-WIV)

Method (Fr)

Scope (Fr)

MS/MS transition (Fr)

Validation file (Fr)

04/08/2010

Multiresidue determination of pesticides in matrices of animal origin by means of GC-MS/MS and UPLC-MS/MS (by ISP-WIV)

Method (Fr)

Scope (Fr)

MS/MS transition (Fr)

Validation dossier (Fr)


Top of the page    



Polycyclic aromatic hydrocarbons (PAH)

Date Subject Documents
31/12/2013 Determination of PAH by GC-MS (by CART)

Method (Fr)

Validation file (Fr)

31/01/2013 Determination of PAH by HPLC-UV/FLD (by WIV-ISP)
 

Method (Fr)

Validation file (Fr)


Top of the page    



Detection of inhibitors in raw milk

Date Subject Documents
10/08/2012

Validation of post screening tests applied in the procedure of the interprofessional organizations for the screening of antimicrobials in milk

Validation dossier (PDF)

06/01/2012

Validation report of the Delvotest T

Validation dossier (PDF)

14/10/2011

Evaluation of the Eclipse 3G

Validation dossier (PDF)

26/08/2011

Validation of the Charm Blue Yellow II

Validation dossier (PDF)


Top of the page    



Veterinary drugs residues

Date Subject Documents
02/06/2017 Screening of veterinary drugs in feed by LC-MS/MS (by CER)

Method (Fr)

Validation file (Fr)

24/06/2016

Detection and confirmation of Antibiotics in poultry manure by LC-MS/MS (D,I)

Methode (Fr)

Validatiedossier   (Fr)

24/06/2016

Detection and confirmation of Aminoglycosides in poultry manure by LC-MS/MS

Methode (Fr)

Validatiedossier (Fr)

23/12/2014 Qualitative test for the detection of inhibitory substances in meat : Explorer V2.0 (by ILVO T&V)

Validation file (PDF)

10/12/2014 Detection, identification and quantification of metabolites of carbadox and olaquindox in muscle tissue from chicken and pork by LC-MS/MS (by CER)

Method (Fr)

Validation file (Fr)

24/03/2014 Detection, identification and quantification of avermectines and other anthelmintiques in animal tissue by LC-MS/MS (validation: partim diflubenzuron in fish, by CER)

Method (Fr)

Validation file (Fr)

10/03/2014 Detection, confirmation and quantification of aminoglycosides in feed by LC-MS/MS (by CER)

Method (Fr)

Validation file (Fr)

07/03/2014 Detection and identification of residues of triphenylmethane dyes  in aquacultural products by LC-MS/MS (by CER)

Method (Fr)

Validation file (Fr)

31/01/2014 Detection, identification and quantification of anthelmintiques and flukicides in muscle tissue by UHPLC-MS/MS (by CER)

Method (Fr)

Validation file (Fr)

21/12/2012 Determination of cross-contamination by coccidiostats in feed by LC-MS/MS (by ISP-WIV)

Method (Fr)

 

21/12/2012 Determination of coccidiostats in muscle tissue by LC-MS/MS (by ISP-WIV)

Method (Fr)

 

21/12/2012 Determination of cephalosporins in muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

21/12/2012 Determination of aminoglycosides in muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

21/12/2012 Determination of macrolide antibiotics in muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

21/12/2012 Determination of tetracycline in muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

21/12/2012 Determination of Beta-lactam antibiotics in muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

05/12/2012 Quantitative determination of NSAID  muscle tissue by LC-MS/MS (by ISP-WIV)
 

Method (Fr)

Validation file (Fr)

14/09/2011 Determination of anthelmintics in meat by LC-MS/MS
 

Method (Fr)

Validation file (Fr)


Our mission is to preserve the safety and the quality of our food in order to protect humans, animals and plants.

Printable version   |   Last update on 06.06.2017   |   Top of the page


Conditions of use & disclaimer   |   Copyright © 2002- FAVV-AFSCA. All rights reserved.